Colour Fastness to Saliva Test|Purpose|Equipment|Test Specimen|Method.


 PURPOSE
To determine the resistance of the colour of textiles to saliva according to GB/T 18886.

EQUIPMENT 

• Perspirometer
• 11 acrylic-resin or glass plates
• Flat-bottomed dishes
• Oven, maintained at (37±2)C
• Light box with light source D65
• Grey scale for assessing change in colour (ISO 105-A02)
• Grey scale for assessing staining (ISO 105-A03)
• Multifibre adjacent fabric, type DW (ISO 105-F10)
• Chemicals for the saliva solution (see preparation of solution)
• Distilled water, grade 3
• Scale 

PREPARATION OF SOLUTION 

Saliva solution, freshly prepared, containing per litre distilled water:
3.0g Lactic acid (CH3∙CH(OH)∙COOH)
0.2g Carbamide (H2N∙CO∙NH2)
4.5g Sodium Chloride (NaCl)
0.3g Potassium Chloride (KCl)
0.3g Sodium Sulphate (Na2SO4)
0.4g Ammonium Chloride (NH4Cl)
No need to bring the saliva solution to specific pH. 

TEST SPECIMEN 

Two specimens for each colour and material measuring 4 cm x 10 cm.
Details such as labels, badges and drawstrings also need to be tested. If the product is multi-coloured, make sure all colours tested. More test specimens could be required if the product is printed, striped or includes several colours.
If details (including prints) are in contrast colour these need to be tested both against multifibre adjacent fabric and the fabric of which the detail is attached. If not in contrast colour, they need to be tested only against multifibre adjacent fabric.

METHOD
1. Cut specimens measuring 4cm x 10cm.

2. Attach a specimen to multifibre adjacent fabric of the same size, by sewing along one of the shorter (4 cm) sides. The multifibre adjacent fabric should be next to the face side of the fabric.
3. Switch on the oven and preheat pre-heat perspirometer & acrylic plates for 30 min.
4. Place the specimens in a dish with 100 ml of the sweat solutions and thoroughly with the help of glass rod/acrylic plate to wet specimen and multifibre for 30 min.
5. Pour off the excess solutions from specimen by using wringer /glass.
6. Place each specimen between two glass or acrylic plates and place them in the perspirometer. Each perspirometer can hold maximum 10 samples. If less, all 11 plates still have to be placed in the perspirometer. Put a pressure of 12.5 kPa on the perspirometer using the load, lock it and then remove the load. 12.5 kpa pressures must be evenly distributed on the sample surface. Plates must be parallel to each other, inclination of plates due to thick and thin (uneven sample surface) surface must be avoided.
7. Place the perspirometer in the oven for 4 hours at (37±2)°C in upright position.


8. Take out the specimens from the oven and perspirometer. Open out each specimen and dry them in room temperature, not exceeding 60°C, with the specimen only being in contact at the point of the stitching.

RESULTS
Assess cross staining, change in colour and colour staining.

NOTE
*To weigh the specimen and multiply the weight by 50 is an easy way to get correct ratio. E.g. for a specimen which weight 2g, 100ml solution is needed.

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